Safety First – Process Instrumentation Material Considerations

September 28th, 2015 No comments

When specifying flow, pressure, temperature or other wetted process control instrumentation there is a lot that needs to be considered. Flow rates, pressures, temperatures, I/O signals, material selection, etc. In addition to all of this the specifier needs to be concerned with safety, certifications, approvals, material integrity, weld integrity and of course quality. I am writing this to make you aware of an element of the material integrity that should be considered when selecting a device and/or instrumentation supplier – hydrogen embrittlement.

Understanding Hydrogen Embrittlement
Hydrogen embrittlement is a type of material deterioration which can be linked to corrosion and corrosion-control processes. It involves the ingress of hydrogen into a component. Hydrogen, being a small molecule, in some situations readily diffuses through the metal crystal structure where it can accumulate and seriously reduce the ductility and load-bearing capacity. This may lead to cracking and catastrophic brittle failures at stresses below the yield stress of susceptible materials. Hydrogen embrittlement occurs in a number of forms but the common features are an applied tensile stress and hydrogen dissolved in the metal. Examples of hydrogen embrittlement are cracking of weldments or hardened steels when exposed to hydrogen rich environments. Hydrogen embrittlement does not affect all materials equally. The most vulnerable are high-strength steels, titanium alloys and aluminum alloys.

Some process instrumentation use high strength steel fasteners in the assembly. A hydrogen rich environment naturally occurs during the zinc plating process that is used to provide corrosion protection for many high strength fasteners. Special care must be taken in the manufacturing process of these high strength fasteners to ensure that they are not susceptible to hydrogen embrittlement.



Eliminating the Risk(s) of Hydrogen Embrittlement
Brooks Instrument eliminates the risk of hydrogen embrittlement by using 18-8 stainless fasteners where possible. The 18-8 stainless fasteners are corrosion resistant and immune to hydrogen embrittlement. All of the fasteners in Brooks Instrument size 0 mass flow devices (ex. SLA5850, 5850E, GF40 mass flow controllers) are 18-8 stainless. In the case where stronger screws are required, Brooks uses high alloy fasteners made by reputable manufacturers with tight control of the manufacturing and plating processes. We also require that all high alloy fasteners go through a high temperature baking process shortly after plating. This baking process drives out all harmful levels of hydrogen from the crystal structure. We also require that our suppliers certify each shipment. Because of these measures, Brooks has never had a field failure due to hydrogen embrittlement.

Brooks Instrument Solid Sense II pressure transducers, with single piece (non-welded) sensor and low internal volume, are proven products not susceptible to hydrogen embrittlement. The sensor was carefully designed with high purity 316L stainless steel material and does not require any internal sensor welding techniques. The Brooks Solid Sense II pressure transducer also utilizes a high temperature annealing process to enhance the sensor robustness ensuring stable performance over time in all gas delivery scenarios. The Brooks Solid Sense II has been selected as the right pressure transducer by gas cabinet manufactures, tool OEMs and end users around the world.

Some competitive pressure transducers have multiple piece designs requiring welding. Impurities introduced during chemical plating and/or welding operations, especially welding of dissimilar materials, may seed nucleation sites. These nucleation sites can result in hydrogen embrittlement which may lead to cracking and/or a change in sensor output. Pressure transducers impacted by hydrogen embrittlement failures could trigger a process or facility safety alarm impacting equipment availability resulting in very expensive maintenance and downtime.

When you are specifying process control instrumentation, be aware of the potential for hydrogen embrittlement and the associated safety concerns. Be sure to ask your suppliers how they minimize the risk of hydrogen embrittlement. Select a supplier that is aware of and has proactively taken steps to minimize the potential for hydrogen embrittlement.

For additional reading on fasteners, see, “The Nuts and Bolts of Bolting,” written by Joe Dille – Lead Mechanical Engineer at Brooks Instrument for over 32 years and published in BMW Motorcycle Owner’s Association – Owners News.

Electronic Pressure Controller Eliminates Droop, Boost and Hysteresis

August 31st, 2015 No comments

Gas pressure control is critical in many applications like life sciences and chemical/petrochemical research where flow is an integral part of the process. Brooks Instrument electronic pressure controllers can be used as they require flow to function. Compared to using a mechanical pressure regulator, electronic pressure controllers eliminate droop, boost and hysteresis, offering stable pressure control.

There are two configurations available for pressure control – upstream and downstream. This terminology is somewhat unique to Brooks Instrument electronic pressure controllers.

Downstream vs. Upstream Pressure Control
Downstream pressure controllers maintain the pressure downstream of the device itself, increasing flow to increase the pressure and decreasing flow to decrease the pressure. For this reason, this is called direct acting. This configuration is commonly called a standard pressure regulator. A downstream pressure controller acts very similar to a typical mass flow controller because they are both direct acting.

Upstream pressure controllers maintain the pressure upstream of the device itself, increasing flow to reduce the pressure and decreasing flow to increase the pressure. For this reason, this is called reverse acting. This configuration is commonly called a back pressure regulator in the industry.


Selecting and Sizing an Electronic Pressure Controller
The following information is required to select and size a Brooks Instrument electronic pressure controller:

1. Process gas
2. Maximum flow rate being used to maintain pressure
-The “sweet spot” for pressure control is between 100 SCCM and 5 SLPM.
3. Calibration pressure (maximum pressure to be controlled)
4. Reference pressure (for upstream controllers the reference pressure is the downstream pressure and for downstream controllers the reference pressure is the upstream pressure)

As long as flow is present in a process you will typically find the need for some type of pressure control. Vessel sizes up to 30 liters commonly use flow rates up to 3 SLPM during their process steps. Brooks Instrument pressure controllers are a perfect fit for these services, offering stable pressure control with no droop, boost or hysteresis, which are commonly experienced when using a mechanical pressure regulator.


Typical Bioreactor Process Using an Upstream Pressure Controller

How do I correct my variable area flow meter for a gas with a different operating density? [FAQs]

September 27th, 2013 Comments off

Now for the “gas” version of the equation…

You want to get a quick flow check on a different gas because the process gas is changing or you might be experimenting with the process, but you don’t have a VA (variable area) flow meter that is calibrated for the different gas.

Enter the necessary information into the equation below and you’ll get the flow rate for the different gas.

Variable Area Flow Meter Gas Correction Equation

Things to Keep in Mind:

  • The meter has to be a size 8 (1/2” nominal size) or larger and of course the flow meter has to be capable of measuring the flow of the different gas.
  • Absolute Scale Unit Conversions:
    • psia = psia + 14.7
    • °R = °F + 460
  • If your experiment is successful, I recommend you get a meter so you don’t have to calculate the flow rate every time you use the different gas.

Visit our Knowledgebase page for more answers to your questions.

Our New GF81 High-Flow MFC Features the Shortest Lay Length on the Market

August 22nd, 2013 Comments off

Our new GF81 High-Flow MFC can be used for gas flow rates up to 300 slpm, making it ideal for high-flow applications in:

  • Thin film
  • Solar
  • Analytical
  • Biotech, and
  • Fuel cell

Here are a few reasons why we’re excited about this new product…

Design Smaller, More Efficient Systems
The compact footprint and low power draw of GF81 allows you to design smaller, more efficient systems. And, with the shortest lay length on the market, installation is easy making GF81 a simple drop-in replacement.


GF81 High-Flow Mass Flow Controller


One Product Series for All Your Process Gases
Since it’s part of our GF40 (elastomer seal) and GF80 (metal seal) Series, the GF81 uses the same high-stability sensor as its low flow siblings, guaranteeing stable, accurate and repeatable mass flow measurement.

The all metal seal flow path allows GF81 to handle almost any gas – including many corrosive and hazardous gases.

An Ideal Upgrade
A wide range of digital and analog I/O options offers the broadest range of communication protocols, making the GF81 an ideal upgrade for existing MFCs or MFMs. Now, you can upgrade to a device that offers better actual process gas accuracy and repeatability over devices that use traditional single-point conversion factors, while keeping the same communication protocols.

Want to Learn More?
The benefits we listed here are only part of the story. There’s more to share about how and why this robust family of devices can be used for a variety of applications.

We’d appreciate the opportunity to talk with you so please, post a comment, email us or call (1-888-554-3569) to speak with one of our flow experts.

How do I correct my variable area flow meter for a liquid with a different operating density? [FAQs]

August 15th, 2013 2 comments

You want to get a quick flow check on a different fluid because the process fluid is changing or you might be experimenting with the process, but you don’t have a VA (variable area) flow meter that is calibrated for the different fluid.


Enter the necessary information into the equation below and you’ll get the flow rate for the different fluid.


variable area flow meter

Correction Equation for Liquid Flow


Things to Keep in Mind:

  • The meter has to be a size 8 (1/2” nominal size) or larger and of course the flow meter has to be capable of measuring the flow of the different fluid.
  • If the new specific gravity is drastically different, the meter may not be capable of registering a flow rate for the new fluid.
  • If your experiment is successful, I recommend you get a meter so you don’t have to calculate the flow rate every time you use the different fluid.


Visit our Knowledgebase page for more answers to your questions.

What I learned at SEMICON West 2013

July 26th, 2013 Comments off

CelerityLogoIt never, ever fails – each time I get out of the office and into the marketplace, I come away with insights and ideas.

At SEMICON West 2013, there was so much to absorb about the industry, suppliers, competitors and customers. But when I hone in on my key insights and what they mean to Brooks Instrument and the people we have the honor of serving, this was numero uno:

What may be old news to us could be “new” news to the marketplace, for a very long time…

Here’s what I mean – back in 2009, Celerity, Inc. joined the Brooks Instrument family. Celerity brought its rich history of growth and innovation in the semiconductor market to Brooks, including well-known mass flow controller brands like:UnitMFC
• Celerity
• Unit
• Millipore
• Mykrolis
• Tylan General

Although we communicated this to the marketplace in a variety of ways, not a single visitor to our booth was aware. That means all of you out there who currently own one of these devices are missing out on getting the best factory certified service for your device as well as the opportunity to upgrade to the latest technology, like our GF100 Series thermal mass flow controllers. This technology platform has been designed to precisely measure, monitor, and control ultra high purity process gas chemistry in semiconductor device manufacturing processes.Mykrolis

We are here for you! If you’d like to know more, email or call us at 1-888-554-3569.

Brooks Featured in Solid State Technology Magazine

June 14th, 2013 Comments off

Our own Shaun Pewsey was quoted extensively in the May issue of Solid State Technology in an article on page 10 titled, “New MFCs Mean Higher Yield.” The article discusses the latest advances in diagnostics for semiconductor production.

Brooks’ new GF135 is featured because it is the first MFC that can test process gas flow without stopping production. Instead of having to take the gas panel offline to run diagnostics, the GF135 uses real-time error detection by momentarily closing the valve. This promises semiconductor manufacturers increased accuracy and increased yield. “In short, the new technology identifies and corrects issues before they happen, preventing wasted time and wasted wafers.”

We hope you enjoy the article. Give it a read here.

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XacTorr CMX guages revealed at SVC TechCon 2013!

April 23rd, 2013 Comments off

Process production can be tricky. In the past, we’ve covered ways to ease the pain of process manufacturing, and today we’re excited to introduce a game-changing development to the industry. Our vacuum measurement expert Ken Tinsley will be presenting a poster session at SVC TechCon 2013 in Providence, R.I., where the XacTorr CMX line of vacuum gauges will take center stage.

The XacTorr CMX line will break new ground, as they’re the first digital capacitance manometers to enter the market. The secret is the Mark-IV sensor built into the gauges. The surface chamber has areas allocated for vapors and particles to group without affecting the sensor. This feature not only extends the sensor life but also increases productivity by reducing the need to re-zero.

Tinsley’s presentation, “Advantages of Digital Calibration in Second Decade of Capacitance Diaphragm Gauges”, will take place today at the Rhode Island Convention Center from 4:00 to 6:00 p.m. As a proud sponsor of the show, we’re offering free admission to anyone interested in learning more about our vacuum technologies. If you’re in the area and would like free admission to the show, simply email your name, company and email address to

We hope to see you at the show!

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Our MT3809 VA Flow Meter is New and Improved!

April 19th, 2013 Comments off

Big news here at Brooks. We’ve got another product launch underway. This one involves a redesign of our MT3809 VA flow meter. That great instrument just got even better.

The new MT3809 works accurately across a staggeringly wide range of operating temperatures — from -50°C to 420°C (-58°F to 780°F) — and at pressures to 1380 bar (20K psi). Even in the most demanding applications measuring gases, liquids, and steam, the MT3809 delivers 2% full-scale/1.6 VDI accuracy. We’ve given the new MT3809 an explosion-proof housing that meets the world’s most stringent hazardous-area classifications, and we’re offering a flameproof option for IIC/Class 1 Division 1 locations.

All in all, you’ve got unprecedented flexibility to use a single flow meter regardless of application, process configuration or flow rate.

Of course we always like to design for value as well as quality and durability, so you can expect the new MT3809 to save you plenty of time and money over the course of its long service life. For starters, installation is fast and easy. That includes retrofitting. Maintenance is simple, too. Weldneck flanges provide long-term durability in all configurations. You don’t need back pressure for gas applications, and we’ve met ASME sealing specifications with a standard gasket, saving you the cost of custom gaskets.

As always, we’d be happy to tell you more about it. Email me, or call us at 1-888-554-3569.

Brooks Team Members Participate in the SolarRun

April 18th, 2013 Comments off

On a sunny Saturday in Holland, team members from Brooks Instrument hit the ground running for the SolarRun, a 5k/10k fun run that benefitted the Solar Without Borders organization.

Brooks Instrument was eager to participate in the event as it helps to increase funding and awareness for Solar Without Borders, a charity that works with a variety of industries to provide photovoltaic panels to hospitals, schools, and orphanages in countries with limited electric infrastructure. Solar Without Borders originally started in West Africa and now operates in numerous countries around the globe including Guatemala, Kenya, and Mongolia.

Poor conditions often exist in hospitals with no or little electricity. Solar panels on these buildings will help to keep medications refrigerated and thus fresh for longer periods of time. Electric lighting also reduces dependence on oil lamps commonly used in maternity wards. The lanterns are known to emit harmful chemicals into the air.

Solar panels can impact literacy rates in impoverished countries. In Burkina Faso, where the literacy rate is only 28.7%, Solar Without Borders hopes to increase literacy by providing electric lighting for children to complete their homework.

The SolarRun is organized by Tempress Systems, a Dutch customer of Brooks Instrument active in the solar industry. Tempress believes strongly that a healthy world is important and they encourage their employees to keep physically fit and to stay energetic. Brooks Instrument shares these values and was excited to both sponsor and participate in the event. Read more…

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